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›› 2020, Vol. 42 ›› Issue (1): 63-69.

• 论文与报告 • 上一篇    下一篇

富含磷脂的南极磷虾油提取工艺研究

胥亚夫1,韩雨哲2,赵月2   

  1. 1. 辽渔南极磷虾科技发展有限公司
    2.
  • 收稿日期:2019-08-15 修回日期:2019-11-20 出版日期:2020-02-25 发布日期:2020-03-02
  • 通讯作者: 胥亚夫

Study on extraction technology of Antarctic krill oil rich in phospholipid

  • Received:2019-08-15 Revised:2019-11-20 Online:2020-02-25 Published:2020-03-02

摘要: 以南极磷虾为原料,采用柠檬酸钠溶液浸泡法从磷虾中提取磷虾油并对其工艺条件进行优化,以提取率、磷脂、酸值和流动性等衡量磷虾油生产成本和产品品质最重要的4个指标综合分析,确定最佳提取工艺条件: 柠檬酸钠溶液浓度1.0%、料液比1∶5、浸泡时间3.0 h。在此工艺条件下,采用95%乙醇浸提磷虾粉,固液分离后,对分离得到的提取液进行减压蒸馏,除去乙醇后得到的磷虾油的磷脂含量为50.15%、酸值为10.33 mgKOH/g,磷虾油的提取率为14.9%, 并且流动性较好。该工艺操作简单,安全实用,提取出的磷虾油磷脂含量高、酸值低、流动性好、品质稳定,极大提高了南极磷虾的综合利用率,具有重要的实际应用价值。

关键词: 南极磷虾, 南极磷虾油, 磷脂, 酸值, 提取率, Antarctic krill, Antarctic krill oil, phospholipid, acid value, extraction ratio

Abstract: Using Antarctic krill as raw material, the pretreatment process of krill was studied by Sodium citrate solution immersion method. Through comprehensive analysis on the most important four aspects of manufacturing cost and product quality of krill oil from extraction rate, phospholipid, acid value and fluidity, the optimum technological conditions were confirmed as follows: the treatment concentration of Sodium citrate solution was 1.0%, the ratio of material-solvent was 1:5, and the soaking time was 3 hours. Under these conditions, krill powder was extracted with 95% ethanol, and the separated extract was distilled under vacuum after solid-liquid separation. After removing ethanol, the phospholipid content and acid value of krill oil can reach 50.15% and 10.33 mg KOH/g respectively, and the extraction rate of krill oil was 14.9%, while its fluidity was excellent. The process was simple in operation, safe and practical, while the extracted krill oil had high phospholipid content, low acid value, good fluidity and stable quality. Therefore, the comprehensive utilization rate of krill was greatly increased, which had important practical application value.

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